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  • Article
  • Open Access

Magnetic Co-Al Layered Double Hydroxides as Peroxymonosulfate Activator for the Removal of Pesticide Multiresidues

  • Zi-Ying Zeng,
  • Cheng-Xiang He,
  • Qin Tian,
  • Jun Long,
  • Bing-Yan Du,
  • Er-Cheng Zhao and
  • Zhong-Hua Yang

The increasing prevalence of multiclass pesticide residues in aquatic environments poses a significant threat to ecosystems and human health. To address this challenge, magnetic Fe3O4@Co5Al-LDH nanoparticles were synthesized as high-performance, easi...

  • Article
  • Open Access

Study of the Dynamic Characteristics of Simulated Droplet Particles in Hydro-Jet Cyclone Based on CFD-DPM

  • Yao Zhang,
  • Yong Yu,
  • Zhi-Bin Zhou,
  • Zheng-Hao Yang,
  • Yu-Long Chang,
  • Li-Wang Wang and
  • Ben-Shuai Guo

The complex behavior of multi-scale droplets in Hydro-jet Cyclone (HJC) systems constrains the parametric study of gas–liquid separation and interfacial transfer. To investigate droplet dynamics at a specific scale in swirling flows, this study...

  • Article
  • Open Access

Coal plays a vital role in energy production, but its combustion releases SO2, causing serious environmental problems. In this study, indigenous microorganisms with sulfur-metabolism potential were isolated from raw coal and evaluated for coal biodes...

  • Article
  • Open Access
96 Views
22 Pages

Intensified Roasting at Low-Temperature and Alkaline Leaching to Efficiently Remove Harmful Elements for Green Utilization of Secondary Aluminum Dross

  • Nianzi Liu,
  • Yilin Wang,
  • Qing Long,
  • Anyan Long,
  • Guihua Liu,
  • Tiangui Qi,
  • Qiusheng Zhou,
  • Leiting Shen and
  • Jian Guo

Secondary aluminum dross (SAD) from the aluminum industry is a hazardous residue that restricts sustainable aluminum production. Residual aluminum nitride (AlN) and insoluble fluorides after conventional pretreatment are major barriers to the safe ut...

  • Article
  • Open Access
130 Views
20 Pages

Ionic liquid-assisted extraction can improve the recovery of monoterpene glycosides from Radix Paeoniae Alba, whereas post-extraction purification and ionic-liquid-associated marker-level quality control remain necessary before further bioactivity ev...

  • Review
  • Open Access
276 Views
28 Pages

Research in the analytical and preparative fields of separation science has a long-standing tradition in the Czech Republic and former Czechoslovakia. Czech and Slovak scientists recognized the advantages of the two most widely used separation techni...

  • Article
  • Open Access
604 Views
15 Pages

This study investigated the effect of ethanol on the relative headspace percent composition of evaporative emissions from gasoline at different temperatures using HS-SPME-GC-MS. The results showed that the relative abundance of monoaromatics in the h...

  • Article
  • Open Access
99 Views
21 Pages

Valorization of Phosphate Tailings into Ca-Mg-Al Layered Double Hydroxides for Phosphate Adsorption from Wastewater

  • Zhe Wang,
  • Hongquan Jing,
  • Bingbing Liu,
  • Yixuan Zhang,
  • Jiangli Li and
  • Cuihong Hou

Phosphate tailings (PTs), a solid waste generated from phosphate flotation, are a low-grade phosphate resource rich in quartz and dolomite. Their long-term accumulation leads to both resource loss and environmental risks, making valorization increasi...

  • Article
  • Open Access
171 Views
9 Pages

212Pb is an important medical radionuclide for targeted alpha therapy, and its reliable supply depends on the efficient production of parent nuclides such as 228Ra, 228Th, and 224Ra. Natural thorium resources are abundant and represent a potential so...

  • Review
  • Open Access
144 Views
40 Pages

Qualitative and quantitative analysis of complex mixtures and structure elucidation is generally impeded by the intrinsic complexity of the NMR spectra and the extensive signal overlap. The conventional approach to characterizing individual metabolit...

  • Article
  • Open Access
191 Views
24 Pages

A novel wide-neck classifier (WNC) was designed to address the problem that thickeners cannot achieve classification prior to flocculation in a single unit. Using the computational fluid dynamics-discrete phase method and PIV experimental method, the...

  • Communication
  • Open Access
179 Views
14 Pages

Metanephrine (MN) and normetanephrine (NMN) are critical biomarkers for neuroendocrine tumors (pheochromocytoma and paraganglioma). Following our previous development of a molecularly imprinted solid-phase extraction (MISPE) sorbent for urine analysi...

  • Article
  • Open Access
255 Views
12 Pages

A Method for Purifying Pseudorabies Virus for Labeling the Neural Circuit by Using CaptoTM Core 700

  • Rui Mei,
  • Qinghan Wang,
  • Kangyixin Sun,
  • You Hu,
  • Fuqiang Xu and
  • Fan Jia

Background: Viral vectors are indispensable tools in gene therapy and neural circuit mapping, offering promising therapeutic strategies for diverse genetic diseases and advancing neuroscience research. To achieve high transduction efficiency while mi...

  • Article
  • Open Access
178 Views
17 Pages

Surface Chemical Regulation of Coal Gangue–Rice Husk Biochar for Concurrent Promotion of Hg2+ Adsorption and Inhibition of Hg0 Production

  • Kaikai Zhang,
  • Wen Ye,
  • Shunquan Shi,
  • Jiale Yang,
  • Yuyu Zhang,
  • Ping Hou,
  • Feng Xie,
  • Yujie He,
  • Jinze Zhao and
  • Shaogang Hu

Mercury (Hg) is a global pollutant that poses a serious threat to ecosystems and human health. Biochar has shown great potential for mercury removal due to its porous structure and abundant surface functional groups. However, redox-active moieties on...

  • Review
  • Open Access
407 Views
40 Pages

Amid growing pressure to reduce carbon emissions, carbon capture, utilization, and storage (CCUS) has become an important pathway toward deep decarbonization. However, the conventional separated “capture–release–conversion” pr...

  • Article
  • Open Access
221 Views
19 Pages

Green Synthesis of Thiourea-Grafted Activated Carbon for Efficient Adsorption of AuCl4

  • Tianyi Chen,
  • Xudong Liu,
  • Yaobin Lai,
  • Jiayi Zan and
  • Xuxia Zhang

The thiourea grafting method can effectively improve the ability of activated carbon to recover chloroauric acid (AuCl4). Conventional grafting strategies rely on acyl halide reactions using reagents such as SOCl2 and CH2Cl2, which suffer from...

  • Article
  • Open Access
156 Views
24 Pages

Identification of Key Aroma-Active Compounds in Plum, Jujube, and Grape Extracts via GC×GC-O-TOF-MS, GC-MS, Aroma Recombination and Omission Tests

  • Ruiyang Chen,
  • Qinghui Jia,
  • Anzhen Fu,
  • Fan Yang,
  • Yixin Dai,
  • Jingzhe Sun,
  • Liya Liu,
  • Ye Liu and
  • Shuang Bi

Fruity natural flavors are widely used in food, cosmetics, and tobacco products, and their flavor profiles directly affect the sensory quality of the final products. However, the volatile organic compound systems in these flavors are highly complex,...

  • Article
  • Open Access
310 Views
18 Pages

Breaking Recovery Bottlenecks in Long-Chain Dicarboxylic Acid Extraction: Effect of pH and Solvents

  • Priyanka Mondal,
  • Iris Cornet,
  • Inge Noëlle Adrienne Van Bogaert,
  • Anita Buekenhoudt and
  • Kristien De Sitter

Efficient recovery of long-chain dicarboxylic acids (LCDAs) from aqueous fermentation broths is a key challenge for the industrial development of bio-based LCDA production. This study evaluates liquid–liquid extraction (LLE) as a downstream rec...

  • Article
  • Open Access
158 Views
21 Pages

In contemporary research on natural bioactive compounds, increasing emphasis is placed on the development of efficient and sustainable extraction technologies. This study aimed to develop and optimize an innovative extraction process for wild cyclame...

  • Article
  • Open Access
244 Views
17 Pages

Hydrophobically Modified Anionic Polyacrylamide for Flocculation–Dewatering of Low-Rank Ultrafine Flotation Clean Coal

  • Qiming Zhuo,
  • Rong Zou,
  • Xuan Du,
  • Leilei Gao,
  • Hongxiang Xu,
  • Jiushuai Deng,
  • Wenli Liu,
  • He Zhang and
  • Kejia Ning

Low-rank ultrafine flotation clean coal typically yields filter cake moisture above 20% due to abundant oxygen-containing functional groups and strong surface hydrophilicity. Conventional polyacrylamide (PAM) flocculants are hydrophilic and improve d...

  • Article
  • Open Access
475 Views
23 Pages

Multi-Objective Optimization of a Cyclone Separator for Improved Separation Efficiency and Reduced Pressure Drop Using CFD and NSGA-II

  • Héctor Calvopiña,
  • Wilson Pavón,
  • Kevin Chacha,
  • Eduardo Bazurto,
  • Aleph Salvador Acebo Arcentales and
  • Angel Fabian Moreira Romero

This study aims to optimize the performance of cyclone separators by simultaneously maximizing separation efficiency and minimizing pressure drop through a CFD-based multi-objective optimization framework. The research objectives are explicitly focus...

  • Article
  • Open Access
233 Views
14 Pages

Dialysis is a widely used and effective method for removing urea from protein solutions, particularly following protein denaturation or solubilization. Due to its small molecular weight (~60 Da), urea can pass through semipermeable membranes, while l...

  • Review
  • Open Access
163 Views
21 Pages

As eutrophication worsens, countries including China, the US, France, Sweden, and South Korea have tightened phosphorus (P) discharge limits for wastewater treatment plants (WWTPs). This paper first reviews China’s evolving P regulations, then...

  • Article
  • Open Access
252 Views
18 Pages

Rapid Quantification of Low-Level Crystalline Impurities in Dalmelitinib Mesylate Using NIR Spectroscopy and Chemometric Modeling

  • Runxi Gui,
  • Xiaogang Lian,
  • Maolin Li,
  • Mingdi Liu,
  • Lina Zhou,
  • Songgu Wu and
  • Qiuxiang Yin

Accurate measurement and control of impurities are critical for ensuring the quality and therapeutic performance of solid-state pharmaceutical formulations. This study introduces a rapid, minimal sample preparation analytical approach for quantifying...

  • Article
  • Open Access
177 Views
14 Pages

Optimization of Subcritical Water Extraction for Artemisia argyi Leaf Polysaccharides Using a Hybrid RSM–NN–DSA Framework

  • Huanping Zhang,
  • Huichao Lv,
  • Xue Gao,
  • Shuhong Wang,
  • Jinhong Song,
  • Yang Jiao and
  • Rongrong Cai

Subcritical water extraction (SWE) is an eco-friendly and efficient technique for isolating bioactive ingredients from natural products. To improve the extraction yield of Artemisia argyi leaf polysaccharides (AAPs), a three-stage hybrid optimization...

  • Article
  • Open Access
199 Views
20 Pages

Flotation of Spodumene Against Quartz by Punicines

  • Stéphanie Mireille Tsanang,
  • Atzin Moran Mendoza,
  • Ali Zgheib,
  • Maximilian Hans Fischer,
  • Annett Wollmann,
  • Ursula E. A. Fittschen,
  • Thomas Schirmer and
  • Andreas Schmidt

Five pH- and light-switchable punicine derivatives were investigated as collectors in the flotation of spodumene and quartz. At the natural pH of the minerals, the punicine substituted with a C17 alkyl residue showed the best recovery under daylight...

  • Article
  • Open Access
404 Views
20 Pages

Flavor Changes Through the Fermentation Process of Longmen Rice Vinegar

  • Yibo Bai,
  • Rui Li,
  • Liman Zheng,
  • Yu Zhang,
  • Huanlu Song,
  • Jing Liu,
  • Weining Huo,
  • Wen Nie and
  • Suyan Wan

The flavor profile of Longmen rice vinegar directly influences consumer purchase intention, and understanding its variation during fermentation is crucial for final product quality control. In this study, the flavor dynamics during the fermentation o...

  • Article
  • Open Access
261 Views
22 Pages

Chemical and Sensory Differences Among Coffee Beverages Brewed by Traditional Moka, Espresso, and Kamira, a Novel Italian Brewing Device

  • Giovanna Lo Vecchio,
  • Rosaria Costa,
  • Rossella Vadalà,
  • Laura De Maria,
  • Rita De Pasquale,
  • Giuseppe Tardiolo and
  • Nicola Cicero

The chemical composition and sensory profile of coffee are influenced by brewing method, namely extraction pressure, temperature, contact time, and equipment. This study compared coffee prepared with a traditional moka pot, a conventional espresso ma...

  • Article
  • Open Access
290 Views
13 Pages

Chemical Profiling of Waste Cake from Black Cumin Oil Production

  • Metodi Mladenov,
  • Ina Yotkovska,
  • Milena Nedkova-Shtipska,
  • Irina Karadjova and
  • Galia Gentscheva

The present work investigates the chemical composition of black cumin (Nigella sativa L.) cake obtained as a by-product of cold-pressed oil extraction. The aim of the study is to assess its potential for further utilization and secondary applications...

  • Article
  • Open Access
185 Views
11 Pages

UPLC-Q-Orbitrap-MS/MS for Rapid Characterization of the Chemical Constituents of Atractylodis lancea and Atractylodis macrocephalae

  • Haibo Wang,
  • Duo Chen,
  • Linglang Meng,
  • Haobin Li,
  • Yanbing Lin,
  • Aowei Liu,
  • Xia Huang and
  • Juan Li

Atractylodis lancea (Cangzhu) and Atractylodes macrocephala (Baizhu) are two traditional Chinese medicines with complex chemical compositions. However, a comprehensive comparative analysis of their constituents remains lacking. In this work, an ultra...

  • Article
  • Open Access
178 Views
25 Pages

Spent lithium-ion battery electrolytes contain fluorine-, sulfur-, and phosphorus-bearing toxins, necessitating deep detoxification and directional conversion into C1–C6 light hydrocarbons. To elucidate the specific catalytic roles and sequenti...

  • Editorial
  • Open Access
302 Views
14 Pages

Chromatography represents a cornerstone of modern analytical chemistry, enabling the separation, identification, and quantification of constituents of complex chemical systems. Its development in the Republic of North Macedonia is closely linked to t...

  • Article
  • Open Access
452 Views
13 Pages

This study provides a comprehensive phytochemical and biological evaluation of Acacia nilotica and Acacia seyal samples collected from Khartoum State, Sudan. Methanolic extracts of A. nilotica leaves (SN), A. seyal leaves (TL), and A. nilotica seeds...

  • Article
  • Open Access
572 Views
14 Pages

Carbon dioxide emissions are a major concern for coal-fired power plants. A capture and utilization method is highly demanded. The wastewater generated by a power plant contains a high concentration of Na+. Using wastewater salts to absorb carbon dio...

  • Article
  • Open Access
234 Views
22 Pages

The Formation Mechanism of the Crystal Morphology of Guanidinoacetic Acid: Selective Adsorption of Additives and Solute Diffusion

  • Xin Chen,
  • Yifan Li,
  • Qian Wu,
  • Ting Wang,
  • Na Wang,
  • Lina Zhou,
  • Hongxun Hao and
  • Jingkang Wang

Guanidinoacetic acid (GAA), an important feed additive, shows poor powder properties due to its morphological characteristics. In this study, GAA was employed as a model compound to investigate the regulatory effects of polymeric additives (hydroxypr...

  • Article
  • Open Access
330 Views
31 Pages

Contaminated gas flows are encountered in most industrial processes and require efficient removal of fine dispersed particles of various types and characteristics. Conventional cyclones are widely used under harsh operating conditions; however, their...

  • Article
  • Open Access
264 Views
18 Pages

Method Development for the Quantitative Analysis of Hydrocarbon Impurities in Amine-Based Desulfurization Solvents

  • Qinchuan Xu,
  • Haiyang Wen,
  • Mengna Xu,
  • Chuanlei Liu,
  • Hui Sun,
  • Chao Zhu,
  • Feifei Long and
  • Jingwen Luo

The antifoaming performance of natural gas desulfurization solvents is critical for maintaining product gas quality and ensuring the safe operation of processing units. Hydrocarbon impurities can enter amine solutions through feed-gas entrainment, we...

  • Article
  • Open Access
216 Views
16 Pages

Comparative DFT Study of Hydration Interactions of Representative Flotation Collector Head Groups

  • Shuxun Li,
  • Yuqiong Li,
  • Haibin Li,
  • Wenjie Zhang,
  • Ci Qu,
  • Meiguang Jiang and
  • Xi Yang

During flotation, the hydration behavior of collector head groups plays an important role in determining collector hydrophilicity and interfacial adsorption behavior. However, although computation-assisted flotation studies have extensively investiga...

  • Article
  • Open Access
213 Views
15 Pages

Study on the Flow Field Characteristics and Particle Motion Behavior in the Cylindrical Hydrocyclone

  • Duanxu Hou,
  • Haihao Wang,
  • Daqing Hou,
  • Hongying Zhu,
  • Hongrun Song,
  • Jingyan Zhang and
  • Qingguo Shao

The cylindrical hydrocyclone can be regarded as a special-shaped hydrocyclone comprising entirely cylindrical sections without conical sections, featuring a unique flat-bottom design combined with central discharge, which promotes substantial particl...

  • Article
  • Open Access
378 Views
12 Pages

This work reports a novel dithiophosphinic acid extractant, bis(isobutylphenyl)dithiophosphinic acid (HL), for the mutual separation of Am(III) and Cm(III) and for the separation of trivalent actinides (An(III)) from lanthanides (Ln(III)). The compou...

  • Article
  • Open Access
201 Views
19 Pages

Poorly soluble hydrophobic organic pollutants, such as indole and diethyl phthalate (DEP), are difficult to remove efficiently from complex industrial wastewater due to low solubility and competitive adsorption. In this study, low-rank coal-based act...

  • Article
  • Open Access
288 Views
23 Pages

Fatty alcohols and aliphatic hydrocarbons occur abundantly in nature and serve as critical feedstocks for the surfactant and fuel industries, respectively. However, their industrial-scale separation and purification are significantly hampered by high...

  • Article
  • Open Access
385 Views
16 Pages

The Effects of Outlet Diameter on Particle Movement and Separation Performance of the Cylindrical Hydrocyclone

  • Duanxu Hou,
  • Haihao Wang,
  • Daqing Hou,
  • Hongying Zhu,
  • Hongrun Song,
  • Honghe Deng and
  • Qingguo Shao

The outlet diameter of hydrocyclones is a critical structural parameter that impacts product distribution and separation performance, drawing significant attention. In this paper, the separation efficiency and particle motion behavior in the cylindri...

  • Article
  • Open Access
291 Views
22 Pages

Effects of Hydrocarbons and Ionic Impurities on Foaming and Purification of UDS Desulfurization Solvent

  • Haiyang Wen,
  • Qiyue Zhao,
  • Yaolin Wang,
  • Zhenwu Jiang,
  • Yupeng Cui,
  • Mengna Xu,
  • Chuanlei Liu and
  • Hui Sun

Severe foaming and a significant decrease in desulfurization performance were noted in a novel UDS solvent applied in a natural gas field in western Sichuan, China. The effects of hydrocarbon and ionic impurities on foaming behavior and the purificat...

  • Review
  • Open Access
394 Views
31 Pages

Coal mine methane (CMM) separation faces significant challenges due to high humidity and multicomponent conditions, under which the selective adsorption performance of CH4 is substantially degraded compared with idealized laboratory scenarios. This r...

  • Article
  • Open Access
425 Views
14 Pages

Metal–organic frameworks (MOFs) show great potential for post-combustion carbon capture, yet their practical application is often constrained by challenges such as powder handling difficulties, limited structural stability during shaping proces...

  • Article
  • Open Access
370 Views
15 Pages

Elemental sulfur frequently coexists with organic polysulfides in environmental samples and laboratory sulfurization experiments, complicating the accurate analysis of sulfur speciation. Reliable methods for selective sulfur removal are therefore req...

  • Article
  • Open Access
818 Views
24 Pages

Multidimensional Quality Evaluation of Drying Methods on the Bioactive Components and Antioxidant Activity of Astragalus membranaceus var. mongholicus Slices

  • Feifan Leng,
  • Jiale Wang,
  • Lizhe Hu,
  • Minmin Li,
  • Yongwei Sun,
  • Yonggang Wang,
  • Jieyin Chen,
  • Xiaofeng Dai,
  • Bin Ma and
  • Zhiqiang Kong
  • + 1 author

This study systematically evaluated the effects of five drying methods (sun drying, freeze drying, shade drying, and hot air drying at 40 °C and 60 °C) on the multidimensional quality of Astragalus membranaceus var. mongholicus slices using m...

  • Article
  • Open Access
561 Views
13 Pages

Direct Analysis of Silk Dyes from the Murong Zhi Tomb from the Tang Dynasty Using Desorption Electrospray Ionization High-Resolution Mass-Spectrometry Imaging (DESI-MSI)

  • Qian Yu,
  • Feng Zhang,
  • Wenchao Lv,
  • Yan Wang,
  • Lei Zhong,
  • Wenting Gu,
  • Junmei Liu,
  • Xinyan Liu,
  • Donghui Xu and
  • Nasi Ai
  • + 2 authors

The identification of dyes in ancient textiles is crucial for provenance research and scientific conservation. However, the extremely significant value of these cultural relics necessitates the use of non-destructive analytical techniques. To establi...

  • Editorial
  • Open Access
1,519 Views
20 Pages

Chromatography started to grow in Greece in the 1980s and it has expanded from basic primary separation methods to a sophisticated, multidisciplinary scientific infrastructure operated today by various expert groups distributed in universities and re...

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